PEG of manufacturer-reported Mn of 1000 Da, glycolide, triethylamine (TEA), mesyl chloride, CS A sodium salt from bovine trachea, EDC hydrochloride, NHS, 2-(N-morpholino)ethanesulfonic acid (MES), 11-azido-3,6,9-trioxaundecan-1-amine (ATA), 2-azidoacetic acid, Cp*Ru(cod)Cl, DTT, and sodium nitrate were purchased from Sigma-Aldrich (St. Louis, MO) and used as received. High-performance liquid chromatography (HPLC)–grade tetrahydrofuran (THF), dichloromethane (DCM), and methanol were also purchased from Sigma-Aldrich and used as is. Ultrapure water was obtained from a Millipore Super-Q water system (Billerica, MA). PBS was prepared using preallocated powder from Sigma-Aldrich and ultrapure water.

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